1-(1-benzothiophen-2-yl)ethan-1-amine synthesis
- Product Name:1-(1-benzothiophen-2-yl)ethan-1-amine
- CAS Number:165737-36-0
- Molecular formula:C10H11NS
- Molecular Weight:177.27
![2-Acetylbenzo[b]thiophene](/CAS/GIF/22720-75-8.gif)
22720-75-8
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165737-36-0
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Yield:165737-36-0 75%
Reaction Conditions:
Stage #1: 2-acetyl benzo[b]thiophenewith titanium(IV) isopropylate;ammonia in methanol at 20;Inert atmosphere;
Stage #2: with sodium tetrahydroborate in methanol at 20; for 3 h;Cooling with ice;
References:
Brem, Juergen;Bencze, Laszlo-Csaba;Liljeblad, Arto;Turcu, Mihaela C.;Paizs, Csaba;Irimie, Florin-Dan;Kanerva, Liisa T. [European Journal of Organic Chemistry,2012,# 17,p. 3288 - 3294] Location in patent:experimental part
![1-BENZO[B]THIOPHEN-2-YL-ETHANOL](/CAS/GIF/51868-95-2.gif)
51868-95-2
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$302.39/250MG
165737-36-0
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