[1,1'-Biphenyl]-4,4'-dicarboxylic acid, 2-nitro- synthesis
- Product Name:[1,1'-Biphenyl]-4,4'-dicarboxylic acid, 2-nitro-
- CAS Number:1314484-59-7
- Molecular formula:C14H9NO6
- Molecular Weight:287.22
1007568-39-9
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1314484-59-7
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Yield:1314484-59-7 74%
Reaction Conditions:
Stage #1: dimethyl 2-nitro-[1,1’-biphenyl]-4,4’-dicarboxylatewith potassium hydroxide in tetrahydrofuran;water; for 20 h;Reflux;
Stage #2: with hydrogenchloride in water; pH=1;
References:
Gotthardt, Meike A.;Grosjean, Sylvain;Brunner, Tobias S.;Kotzel, Johannes;G?nzler, Andreas M.;Wolf, Silke;Br?se, Stefan;Kleist, Wolfgang [Dalton Transactions,2015,vol. 44,# 38,p. 16802 - 16809] Location in patent:supporting information