ChemicalBook CAS DataBase List 1,1'-Bis(di-tert-butylphosphino)ferrocene

1,1'-Bis(di-tert-butylphosphino)ferrocene synthesis

1synthesis methods

Product Name:1,1'-Bis(di-tert-butylphosphino)ferrocene
CAS Number:84680-95-5
Molecular formula:C26H44FeP210*
Molecular Weight:474.42

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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13716-10-4 Synthesis

13716-10-4
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1,1'-Bis(di-tert-butylphosphino)ferrocene

84680-95-5
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Yield:-

Reaction Conditions:

in hexanecomplex suspended in hexane, chlorodi-tert-butylphosphine added at -78°C, allowed to warm to room temp., stirred for 2 h; hydrolyzed with H2O, hexane layer sepd., dried (MgSO4), filtered, concd., chromd. (Al2O3, petroleum ether/Et2O), solvent removed, obtained impure;

References:

Cullen, William R.;Kim, Tae-Jeong;Einstein, Frederick W. B.;Jones, Terry [Organometallics,1983,vol. 2,# 6,p. 714 - 719]

1,1'-Bis(di-tert-butylphosphino)ferrocene Related Search:

1,1'-Bis(diphenylphosphino)ferrocene 1,2,3,4,5-PENTAPHENYL-1'-(DI-TERT-BUTYLPHOSPHINO)FERROCENE TERT-BUTYLDIISOPROPYLPHOSPHINE TRIISOPROPYLPHOSPHINE Di-tert-butylphosphine 1,1'-Bis (di-t-butylphosphino)ferrocene palladium dichloride, Ferrocene