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ChemicalBook CAS DataBase List 1,1-BIS(DIPHENYLPHOSPHINO)ETHYLENE

1,1-BIS(DIPHENYLPHOSPHINO)ETHYLENE synthesis

6synthesis methods
14633-92-2 Synthesis
Phosphine sulfide,1,1'-methylenebis[1,1-diphenyl-

14633-92-2
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) n-BuLi / 1.) benzene, hexane, 30 min, 2.) reflux, 4 h
2: 88 percent / Si2Cl6 / benzene / Heating

References:

Goli;Grim [Tetrahedron Letters,1991,vol. 32,# 30,p. 3631 - 3634]

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