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139185-47-0

1,1-Dichloro-4,4-dimethylpent-2-yne synthesis

4synthesis methods
-

Yield:139185-47-0 1.18 g

Reaction Conditions:

with phosphorus pentachloride in dichloromethane at -20;

References:

Liu, Zheng-Li;Yang, Chao;Xue, Qi-Yan;Zhao, Meng;Shan, Cui-Cui;Xu, Yun-He;Loh, Teck-Peng [Angewandte Chemie - International Edition,2019,vol. 58,# 46,p. 16538 - 16542][Angew. Chem.,2019,vol. 131,p. 16690 - 16694,5] Location in patent:supporting information