ChemicalBook CAS DataBase List 1,1-DIMETHYL-1,2,3,4-TETRAHYDROISOQUINOLINE

1,1-DIMETHYL-1,2,3,4-TETRAHYDROISOQUINOLINE synthesis

3synthesis methods

Product Name:1,1-DIMETHYL-1,2,3,4-TETRAHYDROISOQUINOLINE
CAS Number:41565-85-9
Molecular formula:C11H15N
Molecular Weight:161.24

65185-58-2
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1,1-DIMETHYL-1,2,3,4-TETRAHYDROISOQUINOLINE

41565-85-9
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 20 °C
2: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 3 h / 110 °C / Inert atmosphere
3: hydrogen; trifluorormethanesulfonic acid / dichloromethane / 20 °C
4: sodium hydroxide / methanol / 20 °C

References:

WO2021/55630,2021,A1

Phosphonic diamide, P-[3,4-dihydro-1,1-dimethyl-2(1H)-isoquinolinyl]-N,N,N',N'-tetramethyl- (9CI)

78702-71-3
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41565-85-9
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References

N-(2-bromophenethyl)-2,2,2-trifluoroacetamide

1057246-44-2
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41565-85-9
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References

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