1,2,4-Triazin-3-amine, N-butyl- synthesis
1synthesis methods
- Product Name:1,2,4-Triazin-3-amine, N-butyl-
- CAS Number:1189537-71-0
- Molecular formula:C7H12N4
- Molecular Weight:152.2
Yield:1189537-71-0 53%
Reaction Conditions:
with copper(I) 2-hydroxy-3-methylbenzoate;palladium diacetate;caesium carbonate;4,5-bis(diphenylphosphino)-9,9-dimethylxanthene in toluene at 170; for 2 h;Microwave irradiation;Sealed vial;Buchwald-Hartwig reaction;
References:
Pellegatti, Laurent;Vedrenne, Emeline;Leger, Jean-Michel;Jarry, Christian;Routier, Sylvain [Synlett,2009,# 13,p. 2137 - 2142] Location in patent:experimental part