1-(2,6-DIMETHYLPHENYL)-1H-PYRROLE-3-CARBALDEHYDE synthesis
- Product Name:1-(2,6-DIMETHYLPHENYL)-1H-PYRROLE-3-CARBALDEHYDE
- CAS Number:132688-31-4
- Molecular formula:C13H13NO
- Molecular Weight:199.25
15898-23-4
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2700-30-3
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30186-42-6
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132688-31-4
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Yield:30186-42-6 12 %Spectr. ，132688-31-4 88 %Spectr.
Reaction Conditions:
Stage #1: 1-(2,6-dimethylphenyl)-1H-pyrrole;N,N-diisorpopylformamidewith trichlorophosphate in 1,1-dichloroethane; for 1 h;Reflux;Vilsmeier-Haack reaction;
Stage #2: with potassium hydroxide in 1,1-dichloroethane;water; for 0.0166667 h;regioselective reaction;
References:
Ilyin, Petrv.;Pankova, Alenas.;Kuznetsov, Mikhail A. [Synthesis,2012,vol. 44,# 9,p. 1353 - 1358] Location in patent:experimental part
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30186-42-6
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132688-31-4
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15898-23-4
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607-00-1
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30186-42-6
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132688-31-4
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$140.00/500mg
15898-23-4
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52008-97-6
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30186-42-6
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132688-31-4
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$140.00/500mg
15898-23-4
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93-61-8
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30186-42-6
2 suppliers
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132688-31-4
16 suppliers
$140.00/500mg