1,2-BIS(METHOXYMETHOXY)BENZENE synthesis
1synthesis methods
- Product Name:1,2-BIS(METHOXYMETHOXY)BENZENE
- CAS Number:3688-89-9
- Molecular formula:C10H14O4
- Molecular Weight:198.22
Yield:3688-89-9 90%
Reaction Conditions:
Stage #1: benzene-1,2-diolwith sodium hydride in tetrahydrofuran;N,N-dimethyl-formamide at 20; for 1 h;
Stage #2: chloromethyl methyl ether in tetrahydrofuran;N,N-dimethyl-formamide at 20; for 18 h;Further stages.;
References:
Kiehne, Ulf;Luetzen, Arne [European Journal of Organic Chemistry,2007,# 34,p. 5703 - 5711]