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ChemicalBook CAS DataBase List 1,2-DIBROMO-4-ETHYLBENZENE
134940-69-5

1,2-DIBROMO-4-ETHYLBENZENE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 85 percent / NaBH4 / propan-2-ol / Ambient temperature
2: 84 percent / PBr3 / CHCl3 / -10 deg C to r. t.
3: 80 percent / NaOH, NaBH4 / H2O; various solvent(s) / 5 h / 50 °C

References:

Beck, Anton;Mangold, Klaus-Michael;Hanack, Michael [Chemische Berichte,1991,vol. 124,# 10,p. 2315 - 2321]