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1,2-Ethanediol, 1-(2,4,6-trimethylphenyl)- synthesis

2synthesis methods
769-25-5 Synthesis
2,4,6-TRIMETHYLSTYRENE

769-25-5
87 suppliers
$25.19/1g

1,2-Ethanediol, 1-(2,4,6-trimethylphenyl)-

354153-47-2
5 suppliers
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Yield:354153-47-2 91%

Reaction Conditions:

Stage #1: 2,4,6-trimethylstyrenewith water;cyclopropane-1,1-dicarbonyl peroxide in chloroform at 40; for 24 h;
Stage #2: with water;sodium hydroxide at 60; for 4 h;

References:

Griffith, James C.;Jones, Kevin M.;Picon, Sylvain;Rawling, Michael J.;Kariuki, Benson M.;Campbell, Matthew;Tomkinson, Nicholas C. O. [Journal of the American Chemical Society,2010,vol. 132,# 41,p. 14409 - 14411] Location in patent:supporting information; experimental part