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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 1-(2-hydroxy-3,4,5,6-tetramethoxyphenyl)ethanone
3162-28-5

1-(2-hydroxy-3,4,5,6-tetramethoxyphenyl)ethanone synthesis

14synthesis methods
Obtained by partial demethylation of 2,3,4,5,6-pentamethoxyacetophenone (I),.
Ethanone, 1-(2,3,4,5,6-pentamethoxyphenyl)-

14786-40-4
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1-(2-hydroxy-3,4,5,6-tetramethoxyphenyl)ethanone

3162-28-5
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Yield:3162-28-5 96%

Reaction Conditions:

with boron trichloride in dichloromethane at -78 - -15; for 3 h;regioselective reaction;

References:

Oshitari, Tetsuta;Okuyama, Yuji;Miyata, Yoshiki;Kosano, Hiroshi;Takahashi, Hideyo;Natsugari, Hideaki [Bioorganic and Medicinal Chemistry Letters,2011,vol. 21,# 15,p. 4540 - 4544] Location in patent:scheme or table

Pentamethoxybenzene

13909-75-6
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75-36-5 Synthesis
Acetyl chloride

75-36-5
591 suppliers
$17.92/100G

1-(2-hydroxy-3,4,5,6-tetramethoxyphenyl)ethanone

3162-28-5
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References
Pentamethoxybenzene

13909-75-6
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1-(2-hydroxy-3,4,5,6-tetramethoxyphenyl)ethanone

3162-28-5
6 suppliers
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References
481-53-8 Synthesis
Tangeretin

481-53-8
305 suppliers
$6.00/5mg

1-(2-hydroxy-3,4,5,6-tetramethoxyphenyl)ethanone

3162-28-5
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References
1-(2-hydroxy-3,4,6-trimethoxy-phenyl)ethanone

7507-98-4
7 suppliers
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1-(2-hydroxy-3,4,5,6-tetramethoxyphenyl)ethanone

3162-28-5
6 suppliers
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References