1-(2-(Phenanthren-9-yl)phenyl)propan-2-one synthesis
- Product Name:1-(2-(Phenanthren-9-yl)phenyl)propan-2-one
- CAS Number:1013933-56-6
- Molecular formula:C23H18O
- Molecular Weight:310.39
21906-31-0
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Yield:1013933-56-6 82%
Reaction Conditions:
Stage #1: 1-(2-bromophenyl)propane-2-onewith tetrakis(triphenylphosphine) palladium(0) in 1,2-dimethoxyethane at 20; for 0.333333 h;Inert atmosphere;Suzuki coupling;
Stage #2: 9-phenanthrenylboronic acid in 1,2-dimethoxyethane;ethanol; for 8 h;Reflux;Inert atmosphere;Suzuki coupling;
References:
Xu, Daiwang;Duan, Yazhen;Blair, Ian A.;Penning, Trevor M.;Harvey, Ronald G. [Organic Letters,2008,vol. 10,# 6,p. 1059 - 1062] Location in patent:supporting information; experimental part