(1,3,3-triMethylcyclohexyl)MethanaMine synthesis
- Product Name:(1,3,3-triMethylcyclohexyl)MethanaMine
- CAS Number:53060-57-4
- Molecular formula:C10H21N
- Molecular Weight:155.28
7027-11-4
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53060-57-4
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: 99 percent / NaBH4 / methanol / 0.5 h / 0 - 20 °C
2.1: Et3N / CH2Cl2 / 1 h / 0 - 20 °C
3.1: 2,6-lutidine / 1.5 h / 200 °C
3.2: H2 / Pd/C / methanol
4.1: LiAlH4*AlCl3 / diethyl ether
References:
Dischino, Douglas D.;Cianci, Christopher;Krystal, Mark;Meanwell, Nicholas A.;Morimoto, Hiromi;Pearce, Bradley C.;Williams, Philip;Yu, Kuo-Long [Journal of labelled compounds and radiopharmaceuticals,1999,vol. 42,# 10,p. 965 - 974]
78-59-1
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53060-57-4
14 suppliers
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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53060-57-4
14 suppliers
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72641-05-5
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53060-57-4
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1000210-73-0
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53060-57-4
14 suppliers
$650.00/1g