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ChemicalBook CAS DataBase List 1,3,5-tribroMo-2-chlorobenzene
78904-10-6

1,3,5-tribroMo-2-chlorobenzene synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 99 percent / i-pentyl nitrite; HOAc / 0 - 5 °C
2: 92 percent / aq. NaOH / 0.5 h / 0 - 5 °C
3: 78 percent / Et3PhCH2N(+)Cl(-); MeSO3H; Cu / acetonitrile / 1 h / 40 °C

References:

Barbero;Degani;Diulgheroff;Dughera;Fochi [Synthesis,2001,# 14,p. 2180 - 2190]