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ChemicalBook CAS DataBase List 1-(3-acetyl-5-nitrophenyl)ethanone
87533-54-8

1-(3-acetyl-5-nitrophenyl)ethanone synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) Mg, CCl4 / 1.) EtOH, Et2O, 3 h, 2.) EtOH, Et2O, THF, reflux, 16 h
2: 65 percent / H2SO4 / acetic acid; H2O / 3.5 h / Heating

References:

Ulrich, Peter;Cerami, Anthony [Journal of Medicinal Chemistry,1984,vol. 27,# 1,p. 35 - 40]