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ChemicalBook CAS DataBase List 1-(3-Bromopyridin-2-yl)ethanol
1383734-83-5

1-(3-Bromopyridin-2-yl)ethanol synthesis

2synthesis methods
-

Yield:1383734-83-5 52%

Reaction Conditions:

Stage #1: 3-Bromopyridinewith 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex in tetrahydrofuran at 0; for 3 h;
Stage #2: acetaldehyde in tetrahydrofuran at 20; for 1.5 h;

References:

Subota, Andrii I.;Lutsenko, Anton O.;Vashchenko, Bohdan V.;Volochnyuk, Dmitriy M.;Levchenko, Vitalina;Dmytriv, Yurii V.;Rusanov, Eduard B.;Gorlova, Alina O.;Ryabukhin, Sergey V.;Grygorenko, Oleksandr O. [European Journal of Organic Chemistry,2019,vol. 2019,# 22,p. 3636 - 3648]