1-(3-Chlorophenyl)prop-2-yn-1-one synthesis
- Product Name:1-(3-Chlorophenyl)prop-2-yn-1-one
- CAS Number:33899-25-1
- Molecular formula:C9H5ClO
- Molecular Weight:164.59
587-04-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 - 20 °C / Inert atmosphere
2.1: potassium carbonate / methanol / 2 h / 20 °C / Inert atmosphere
3.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere
References:
Ge, Guang-Cun;Mo, Dong-Liang;Ding, Chang-Hua;Dai, Li-Xin;Hou, Xue-Long [Organic Letters,2012,vol. 14,# 22,p. 5756 - 5759]
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33899-25-1
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