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ChemicalBook CAS DataBase List 1,3-diazidobenzene
13556-50-8

1,3-diazidobenzene synthesis

3synthesis methods
-

Yield:13556-50-8 60%

Reaction Conditions:

Stage #1: benzene-1,3-diaminewith sulfuric acid;NaNO2 in lithium hydroxide monohydrate at 0 - 2;
Stage #2: with Caswell No. 744A in lithium hydroxide monohydrate at 0 - 5;

References:

Chapyshev, Sergei Viktorovich;Tomioko, Hideo [Bulletin of the Chemical Society of Japan,2003,vol. 76,# 11,p. 2075 - 2090]

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