1,4,7,10,13,16-HEXAAZACYCLOOCTADECANE synthesis
- Product Name:1,4,7,10,13,16-HEXAAZACYCLOOCTADECANE
- CAS Number:296-35-5
- Molecular formula:C12H30N6
- Molecular Weight:258.41
4439-20-7
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296-35-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 72 percent / 30percent NaOH / triethylbenzylammonium chloride / H2O; CH2Cl2 / 10 - 15 °C
2: 85 percent / 5percent NaOH / tetrabutylammonium iodide / H2O; toluene / Heating; 8-10 h
3: 75 percent / conc. H2SO4 / 100 - 105 °C / Heating; 50-70 h
References:
Luk'yanenko, N. G.;Basok, S. S.;Filonova, L. K.;Kulikov, N. V.;Pastushok, V. N. [Chemistry of Heterocyclic Compounds,1990,vol. 26,# 3,p. 346 - 349][Khimiya Geterotsiklicheskikh Soedinenii,1990,# 3,p. 401 - 404]
56187-09-8
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296-35-5
67 suppliers
$143.00/250 mg
52601-75-9
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56234-52-7
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296-35-5
67 suppliers
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55442-07-4
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296-35-5
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