1,4-Benzenedicarboxaldehyde, 2,3-dihydroxy- synthesis
- Product Name:1,4-Benzenedicarboxaldehyde, 2,3-dihydroxy-
- CAS Number:148063-59-6
- Molecular formula:C8H6O4
- Molecular Weight:166.13
120-80-9
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetone / 12 h / Reflux
2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether / 18 h / Reflux
2.2: 12 h / 20 °C
3.1: boron tribromide / dichloromethane / 4 h / 20 °C
References:
Hiremath, Uma S. [Tetrahedron Letters,2013,vol. 54,# 26,p. 3419 - 3423]
179693-85-7
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91-16-7
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