1,4-bis(4-nitrosophenyl)piperazine synthesis
- Product Name:1,4-bis(4-nitrosophenyl)piperazine
- CAS Number:4963-30-8
- Molecular formula:C16H16N4O2
- Molecular Weight:296.32
613-39-8
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Yield:4963-30-8 0.481 g
Reaction Conditions:
Stage #1: 1,4-diphenyl-piperazinewith hydrogenchloride;sodium nitrite in water at 0; for 0.166667 h;
Stage #2: with triethylamine in methanol;
References:
Wirth, Stefan;Barth, Florian;Lorenz, Ingo-Peter [Dalton Transactions,2012,vol. 41,# 7,p. 2176 - 2186] Location in patent:experimental part