1,4-DIMETHOXY-2,3-DIBROMOBENZENE synthesis
- Product Name:1,4-DIMETHOXY-2,3-DIBROMOBENZENE
- CAS Number:5030-61-5
- Molecular formula:C8H8Br2O2
- Molecular Weight:295.96
1207434-10-3
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Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere
1.2: -78 - 25 °C / Inert atmosphere
2.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 0 - 25 °C / Inert atmosphere
3.1: potassium carbonate / acetone / 18 h / Reflux
4.1: isopropylmagnesium chloride / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere
4.2: -78 - 25 °C / Inert atmosphere
5.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 0 - 25 °C / Inert atmosphere
6.1: potassium carbonate / acetone / 18 h / Reflux
References:
Diemer, Vincent;Leroux, Frederic R.;Colobert, Fracoise [European Journal of Organic Chemistry,2011,# 2,p. 327 - 340]
1266379-51-4
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74-88-4
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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5030-61-5
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1000210-73-0
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5030-61-5
50 suppliers
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1000210-73-0
0 suppliers
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5030-61-5
50 suppliers
$37.00/100mg