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1-(4-methylphenyl)prop-2-yn-1-one synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: tetrahydrofuran / 0 - 20 °C
2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 5 h

References:

Shen, Yang;Cai, Shuying;He, Chi;Lin, Xufeng;Lu, Ping;Wang, Yanguang [Tetrahedron,2011,vol. 67,# 43,p. 8338 - 8342]