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ChemicalBook CAS DataBase List 1-(4-Phenoxyphenoxy)-2-propanol
57650-78-9

1-(4-Phenoxyphenoxy)-2-propanol synthesis

4synthesis methods
-

Yield: 95%

Reaction Conditions:

with sodium hydroxide in water;toluene at 85; for 0.166667 h;Temperature;Reagent/catalyst;

Steps:

1 Example 2
The specific steps of the synthesis reaction with embodiment 1, in distinction, the 20% sodium hydroxide aqueous solution as the synthesis of the catalyst in the reaction of acid-binding agent, and respectively adopt methanol, toluene, acetonitrile as the reaction solvent. Wherein the reaction temperature of different solvent with different corresponding to the reaction yield as shown in the table below:

References:

Ye, Zhenjun;Wu, Qingyang;Bi, Quang;Fang, Yan;Dong, Jiansheng;Zhang, Zhiping;Kong, Qianguang;Wang, Man;Han, Haiping;Gu, Haohua;Xu, Haiyan;Xu, Yan CN105330519, 2016, A Location in patent:Paragraph 0040; 0045