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ChemicalBook CAS DataBase List 1,5-DI-TERT-BUTYL-1,4-PENTADIYN-3-ONE
35845-67-1

1,5-DI-TERT-BUTYL-1,4-PENTADIYN-3-ONE synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / 0 °C / Inert atmosphere
1.2: 2.08 h / 0 - 20 °C / Inert atmosphere
2.1: manganese(IV) oxide / dichloromethane / 20 °C

References:

Qiu, Yi-Feng;Yang, Fang;Qiu, Zi-Hang;Zhong, Mei-Jin;Wang, Li-Jing;Ye, Yu-Ying;Song, Bo;Liang, Yong-Min [Journal of Organic Chemistry,2013,vol. 78,# 23,p. 12018 - 12028]

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