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1,5-DICHLORO-2,4-DIFLUOROBENZENE synthesis

5synthesis methods
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Yield:-

Steps:

2 Preparation of 1,3-dichloro-4,6-difluorobenzene
At the same time, fresh 5-chloro-2,4-difluoronitrobenzene is added to the reaction in accordance with the quantity of product removed. The yields of 1,3-dichloro-4,6-difluorobenzene are over 90% of theory, based on reacted 5-chloro-2,4-difluoronitrobenzene.

References:

Hoechst Atkiengesellschaft US5294742, 1994, A

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