1,5-naphthylene di(acetate) synthesis
- Product Name:1,5-naphthylene di(acetate)
- CAS Number:605-89-0
- Molecular formula:C14H12O4
- Molecular Weight:244.24
Yield:605-89-0 99%
Reaction Conditions:
with pyridine for 1 h;
Steps:
5.1 Step 1 Synthesis of 5- (acetyloxy) naphthalen-1-yl acetate
Dissolve 1,5-dihydroxynaphthalene (10.0 g, 62.4 mmol) in pyridine, add acetic anhydride (13.4 g, 125 mmol), stir for 1 hour, add water, and collect the precipitated crystals by filtration. Obtained 5.0 g (99%).
References:
JP2019/19076,2019,A Location in patent:Paragraph 0170; 0171
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