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ChemicalBook CAS DataBase List 1,6-DIVINYLPERFLUOROHEXANE

1,6-DIVINYLPERFLUOROHEXANE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 76 percent / dibutyl peroxide / 1.) a) -130 deg C, b) 130 deg C, 22 h
2: 82 percent / KOH / ethane-1,2-diol / 140 °C

References:

Baum, Kurt;Bedford, Clifford D.;Hunadi, Ronald J. [Journal of Organic Chemistry,1982,vol. 47,# 12,p. 2251 - 2257]