1-Acetyl-piperidine-4-carboxylic acid Methyl ester synthesis
- Product Name:1-Acetyl-piperidine-4-carboxylic acid Methyl ester
- CAS Number:126291-66-5
- Molecular formula:C9H15NO3
- Molecular Weight:185.22
25503-90-6
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18107-18-1
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126291-66-5
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Yield:-
Reaction Conditions:
in diethyl ether;
Steps:
5.A
To a solution of l-acetyl^-piperidinecarboxylic acid(1.71g, lOmmol) in 2OmL diethyl ether was added an excess of 2.0 M trimethyisilyldiazomethane. The volatiles were removed in vacuo. The crude residue was triturated to high purity with diethyl ether.
References:
WO2007/81897,2007,A2 Location in patent:Page/Page column 24
2971-79-1
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108-24-7
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126291-66-5
15 suppliers
$298.00/500mg