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ChemicalBook CAS DataBase List 1-BENZOTHIOPHEN-5-YL ISOCYANATE
239097-78-0

1-BENZOTHIOPHEN-5-YL ISOCYANATE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 100 percent / SOCl2, DMF / toluene / 3 h / Heating
2: 100 percent / sodium azide / tetrahydrofuran / 15 h
3: 100 percent / toluene / 1 h / Heating

References:

Murakami, Yasushi;Hara, Hirokazu;Okada, Tetsuo;Hashizume, Hiroshi;Kii, Makoto;Ishihara, Yasunobu;Ishikawa, Michio;Shimamura, Mayumi;Mihara, Shin-Inchi;Kato, Goro;Hanasaki, Kohji;Hagishita, Sanji;Fujimoto, Masafumi [Journal of Medicinal Chemistry,1999,vol. 42,# 14,p. 2621 - 2632]

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