Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 1-BOC-2-CYANO-2-METHYLPIPERIDINE
746658-72-0

1-BOC-2-CYANO-2-METHYLPIPERIDINE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 86 percent / tetrahydrofuran / 48 h
2.1: LDA; dimethylpropyleneurea / tetrahydrofuran; hexane / 1 h / -78 °C
2.2: 90 percent / tetrahydrofuran; hexane / 2 h / -78 °C

References:

Wolckenhauer, Scott A.;Rychnovsky, Scott D. [Organic Letters,2004,vol. 6,# 16,p. 2745 - 2748]