1-chloro-3-tert-butyl-benzene synthesis
- Product Name:1-chloro-3-tert-butyl-benzene
- CAS Number:3972-55-2
- Molecular formula:C10H13Cl
- Molecular Weight:168.66
5369-19-7
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3972-55-2
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Yield:3972-55-2 63%
Reaction Conditions:
Stage #1: 3-tert-butylanilinewith hydrogenchloride;sodium nitrite in water at 0; for 0.5 h;Inert atmosphere;
Stage #2: with hydrogenchloride;copper(l) chloride in water at 0; for 5 h;Inert atmosphere;
References:
Ikemoto, Koki;Kobayashi, Ryo;Sato, Sota;Isobe, Hiroyuki [Angewandte Chemie - International Edition,2017,vol. 56,# 23,p. 6511 - 6514][Angew. Chem.,2017,vol. 129,p. 6611 - 6614] Location in patent:supporting information
253185-04-5
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3972-55-2
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3972-56-3
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$14.00/1g
7073-98-5
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42265-67-8
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$36.00/1g
3972-55-2
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20330-45-4
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$29.00/5g
3972-55-2
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31002-87-6
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$504.13/5MG
3972-55-2
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