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111895-49-9

1-[(E)-but-1-enyl]sulfonyl-4-methyl-benzene synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) lithium diisopropylamide; / 1.) THF, -78 deg C, 1 h; 2.) THF, -78 deg C - room temp., overnight;
2: H2O2 / tetrahydrofuran / 0 deg C - 1 h, room temp. - 2h

References:

Inomata, Katsuhiko;Sasaoka, Shin-ichi;Kobayashi, Toshifumi;Tanaka, Yuhji;Igarashi, Susumu;et al. [Bulletin of the Chemical Society of Japan,1987,vol. 60,p. 1767 - 1780]