1'H-Spiro[cyclopentane-1,2'-quinazoline]-4'-thiol synthesis

1synthesis methods

Product Name:1'H-Spiro[cyclopentane-1,2'-quinazoline]-4'-thiol
CAS Number:346458-41-1
Molecular formula:C12H14N2S
Molecular Weight:218.32

1135-80-4 Synthesis

1'H-Spiro[cyclopentane-1,2'-quinazolin]-4'(3'H)-one

1135-80-4
15 suppliers
$110.00/50mg

1'H-Spiro[cyclopentane-1,2'-quinazoline]-4'-thiol

346458-41-1
8 suppliers
$39.00/1mg

Yield:346458-41-1 89%

Reaction Conditions:

with pyridin-1-ium-1-yl[pyridin-1-ium-1-yl(sulfido)phosphinothioyl]sulfanyl-sulfido-thioxo-phosphane in acetonitrile; for 7 h;Reflux;

References:

Bergman, Jan;Pettersson, Birgitta;Hasimbegovic, Vedran;Svensson, Per H. [Journal of Organic Chemistry,2011,vol. 76,# 6,p. 1546 - 1553] Location in patent:experimental part

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