Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

1-Heptatriacotanol synthesis

3synthesis methods
1-Heptatriacotanol

105794-58-9
2 suppliers
inquiry

-

Yield:-

Steps:

Multi-step reaction with 10 steps
1: sulfuric acid
2: lithium aluminium tetrahydride / tetrahydrofuran
3: 1H-imidazole / N,N-dimethyl-formamide
4: 1H-imidazole; iodine; triphenylphosphine / toluene
5: n-butyllithium; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran
6: hydrogen; palladium on activated charcoal / ethyl acetate
7: pyridinium chlorochromate / dichloromethane
8: sodium hexamethyldisilazane / tetrahydrofuran
9: tetrabutyl ammonium fluoride / tetrahydrofuran
10: hydrogen; palladium 10% on activated carbon / ethyl acetate

References:

Zhang, Hong-Yan;Yamakawa, Yu-Ichiro;Matsuya, Yuji;Toyooka, Naoki;Tohda, Chihiro;Awale, Suresh;Li, Feng;Kadota, Shigetoshi;Tezuka, Yasuhiro [Bioorganic and Medicinal Chemistry Letters,2014,vol. 24,# 2,p. 604 - 608]

FullText