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76413-99-5

1-methoxy-8,9-dihydro-5H-benzo[7]annulen-6(7H)-one synthesis

3synthesis methods
sodium 6-hydroxy-1-methoxy-6,7,8,9-tetrahydro-5H-benzo[7]annulene-6-sulfonate

1427073-90-2
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Yield:76413-99-5 403 mg

Reaction Conditions:

with hydrogenchloride;water in tert-butyl methyl ether;

References:

Purohit, Vikram C.;Allwein, Shawn P.;Bakale, Roger P. [Organic Letters,2013,vol. 15,# 7,p. 1650 - 1653] Location in patent:supporting information