1-METHYL-PROP-2-YNYLAMINE HYDROCHLORIDE synthesis

2synthesis methods

Yield: 3.75 g

Reaction Conditions:

Stage #1:1-methylprop-2-ynyl methanesulfonate with ammonium hydroxide at 20; for 18 h;
Stage #2: with hydrogenchloride at 0;

References:

Song, Hongjian;Liu, Yongxian;Wang, Qingmin [Organic Letters,2013,vol. 15,# 13,p. 3274 - 3277] Location in patent:supporting information

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