1-(Naphthalen-2-yl)ethanaMine HCl synthesis
- Product Name:1-(Naphthalen-2-yl)ethanaMine HCl
- CAS Number:39110-76-4
- Molecular formula:C12H14ClN
- Molecular Weight:207.6993
939-27-5
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39110-76-4
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Yield:39110-76-4 50%
Reaction Conditions:
Stage #1: 2-ethylnaphthalenewith Benzophenone imine;copper(l) iodide;1,10-Phenanthroline;di-tert-butyl peroxide in chlorobenzene at 90; for 48 h;Inert atmosphere;Sealed tube;
Stage #2: with hydrogenchloride in methanol;water;chlorobenzene at 40; for 15 h;Inert atmosphere;Sealed tube;
References:
Kramer, S?ren [Organic Letters,2019,vol. 21,# 1,p. 65 - 69] Location in patent:supporting information
93-08-3
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39110-76-4
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74924-94-0
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39110-76-4
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120342-65-6
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39110-76-4
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![Phosphinic amide, N-[1-(2-naphthalenyl)ethylidene]-P,P-diphenyl-](/CAS/20180527/GIF/82572-08-5.gif)
82572-08-5
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39110-76-4
21 suppliers
$110.00/1g