1-Nitroso-5-(3-pyridinyl)-2-pyrrolidinol acetate synthesis
1synthesis methods
- Product Name:1-Nitroso-5-(3-pyridinyl)-2-pyrrolidinol acetate
- CAS Number:68743-65-7
- Molecular formula:C11H13N3O3
- Molecular Weight:235.24
Yield:68743-65-7 637 mg
Reaction Conditions:
Stage #1: acetic acid;3-(3,4-dihydro-2H-pyrrol-2-yl)-pyridinewith sodium nitrite at 5 - 20; for 1 h;Inert atmosphere;
Stage #2: with water;sodium hydrogencarbonate
References:
Marriner, Gwendolyn A.;Kerwin, Sean M. [Journal of Organic Chemistry,2009,vol. 74,# 7,p. 2891 - 2892] Location in patent:supporting information; experimental part