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1-Oxa-4-thiaspiro[4.6]undecane synthesis

1synthesis methods
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Yield: 89%

Reaction Conditions:

with zirconium(IV) chloride in dichloromethane at 20; for 13 h;Cyclization;Condensation; Monothioacetalization;

References:

Karimi, Babak;Seradj, Hassan [Synlett,2000,# 6,p. 805 - 806]