1-Propanol, 3-(octadecyloxy)-2-(phenylmethoxy)- synthesis

9synthesis methods

Product Name:1-Propanol, 3-(octadecyloxy)-2-(phenylmethoxy)-
CAS Number:86008-21-1
Molecular formula:C28H50O3
Molecular Weight:434.69

112-89-0 Synthesis

112-89-0
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1-Propanol, 3-(octadecyloxy)-2-(phenylmethoxy)-

86008-21-1
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Yield:-

Steps:

Multi-step reaction with 5 steps
1.1: sodium hydride / toluene / Inert atmosphere; Schlenk technique; Reflux
2.1: hydrogenchloride / water; methanol / 2 h / Inert atmosphere; Schlenk technique; Reflux
3.1: pyridine / 16 h / 50 °C / Inert atmosphere; Schlenk technique
4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique
4.2: 20 °C / Inert atmosphere; Schlenk technique
5.1: toluene-4-sulfonic acid / methanol; dichloromethane / 4 h / 20 °C / Inert atmosphere; Schlenk technique

References:

Alam, Md. Maqusood;Hassan, Ahmed H.E.;Lee, Kun Won;Cho, Min Chang;Yang, Ji Seul;Song, Jiho;Min, Kyung Hoon;Hong, Jongki;Kim, Dong-Hyun;Lee, Yong Sup [Bioorganic Chemistry,2019,vol. 84,p. 51 - 62]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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86008-21-1
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References

629-93-6
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$19.00/1g

14690-00-7
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$70.00/250mg

86008-21-1
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References

544-62-7 Synthesis

544-62-7
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86008-21-1
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References

86334-56-7
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86008-21-1
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References