1-PYRIDIN-2-YL-PENT-4-EN-1-OL synthesis
- Product Name:1-PYRIDIN-2-YL-PENT-4-EN-1-OL
- CAS Number:81417-99-4
- Molecular formula:C10H13NO
- Molecular Weight:163.22
1121-60-4
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Yield:81417-99-4 97%
Reaction Conditions:
Stage #1: 1-bromo-4-butenewith magnesium in tetrahydrofuran at 70; for 1 h;Inert atmosphere;
Stage #2: pyridine-2-carbaldehyde in tetrahydrofuran at 0;Inert atmosphere;
Stage #3: with water;ammonium chloride in tetrahydrofuran;Inert atmosphere;
References:
Hardin Narayan, Alison R.;Sarpong, Richmond [Organic and Biomolecular Chemistry,2012,vol. 10,# 1,p. 70 - 78] Location in patent:supporting information; experimental part