(1-PyriMidin-2-ylpiperid-4-yl)MethylaMine, 97% synthesis

2synthesis methods

7144-05-0 Synthesis

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 4-toluenesulfonic acid / toluene / 5 h / Heating
2: Et₃N / toluene / 18 h / 95 °C
3: 5 M aq. HCl / 6 h / 95 °C

References:

Birch, Alan M.;Bradley, Paul A.;Gill, Julie C.;Kerrigan, Frank;Needham, Pat L. [Journal of Medicinal Chemistry,1999,vol. 42,# 17,p. 3342 - 3355]

1722-12-9 Synthesis

7144-05-0 Synthesis

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