10-Octadecenoic acid, (10E)- synthesis
- Product Name:10-Octadecenoic acid, (10E)-
- CAS Number:5684-82-2
- Molecular formula:
- Molecular Weight:0
Yield:5684-82-2 88%
Reaction Conditions:
Stage #1: C13H23BrO2with tert-butylmagnesium chloride in tetrahydrofuran at -78; for 0.166667 h;Inert atmosphere;
Stage #2: pentylmagnesium chloridewith 1-methyl-pyrrolidin-2-one;buta-1,3-diene;nickel dichloride in tetrahydrofuran at 0; for 1 h;Inert atmosphere;
References:
Iwasaki, Takanori;Higashikawa, Kiyokazu;Reddy, Vutukuri P.;Ho, Willbe W. S.;Fujimoto, Yukari;Fukase, Koichi;Terao, Jun;Kuniyasu, Hitoshi;Kambe, Nobuaki [Chemistry - A European Journal,2013,vol. 19,# 9,p. 2956 - 2960] Location in patent:supporting information
2442-70-8
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60-33-3
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5684-82-2
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112-79-8
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506-17-2
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693-72-1
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57-11-4
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