(S)-3-(3-broMophenyl)-4-(4-chlorophenyl)butan-2-one synthesis
- Product Name:(S)-3-(3-broMophenyl)-4-(4-chlorophenyl)butan-2-one
- CAS Number:1002752-54-6
- Molecular formula:C16H14BrClO
- Molecular Weight:337.64
1204241-05-3
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676-58-4
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1002752-54-6
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Yield:1002752-54-6 11.5 kg
Reaction Conditions:
Stage #1: C15H11BrCl2Owith N,O-dimethylhydroxylamine*hydrochloride;potassium carbonate in water at 30; for 1.25 h;Inert atmosphere;Large scale;
Stage #2: methylmagnesium chloride in water;toluene; for 1.5 h;Inert atmosphere;Large scale;
References:
Chen, G-Yi;Frey, Lisa F.;Shultz, Scott;Wallace, Debra J.;Marcantonio, Karen;Payack, Joeseph F.;Vazquez, Enrique;Springfield, Shawn A.;Zhou, George;Liu, Ping;Kieczykowski, Gerard R.;Chen, Alex M.;Phenix, Brian D.;Singh, Utpal;Strine, Jeff;Izzo, Brianne;Krska, Shane W. [Organic Process Research and Development,2007,vol. 11,# 3,p. 616 - 623]
1878-67-7
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941280-51-9
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104-83-6
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