tert-butyl 4-(4-chloro-3-methoxyphenyl)piperazine-1-carboxylate synthesis
- Product Name:tert-butyl 4-(4-chloro-3-methoxyphenyl)piperazine-1-carboxylate
- CAS Number:1010073-85-4
- Molecular formula:C16H23ClN2O3
- Molecular Weight:326.82
16817-43-9
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Yield:1010073-85-4 95%
Reaction Conditions:
with tris-(dibenzylideneacetone)dipalladium(0);2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;sodium t-butanolate in toluene at 60;
References:
Pennell, Andrew M.K.;Aggen, James B.;Sen, Subhabrata;Chen, Wei;Xu, Yuan;Sullivan, Edward;Li, Lianfa;Greenman, Kevin;Charvat, Trevor;Hansen, Derek;Dairaghi, Daniel J.;Wright, J.J. Kim;Zhang, Penglie [Bioorganic and Medicinal Chemistry Letters,2013,vol. 23,# 5,p. 1228 - 1231]