101498-55-9 synthesis

1synthesis methods

Product Name:101498-55-9
CAS Number:101498-55-9
Molecular formula:C15H20O
Molecular Weight:216.32

119-64-2
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638-29-9
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101498-55-9
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Yield: 62%

Reaction Conditions:

Stage #1:n-valeryl chloride with aluminum (III) chloride in 1,2-dichloro-ethane at 0; for 0.166667 h;Friedel-Crafts Acylation;
Stage #2:tetralin in 1,2-dichloro-ethane at 50; for 2 h;Friedel-Crafts Acylation;

References:

Siddaraju, Yogesh;Prabhu, Kandikere Ramaiah [Organic and Biomolecular Chemistry,2015,vol. 13,# 24,p. 6749 - 6753] Location in patent:supporting information

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