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1033743-83-7

3-(4-Boc-Piperazin-1-ylsulfonyl)phenylboronic acid pinacol ester synthesis

3synthesis methods
937014-80-7 Synthesis
4-Boc-1-[(3-Bromobenzene)sulfonyl]piperazine

937014-80-7
23 suppliers
$20.00/1g

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Yield:1033743-83-7 9.1 g

Reaction Conditions:

with dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2;potassium acetate in 1,2-dimethoxyethane at 90; for 2 h;Suzuki-Miyaura cross-coupling;

References:

Leahy, James W.;Buhr, Chris A.;Johnson, Henry W. B.;Kim, Byung Gyu;Baik, Taegon;Cannoy, Jonah;Forsyth, Timothy P.;Jeong, Joon Won;Lee, Matthew S.;Ma, Sunghoon;Noson, Kevin;Wang, Longcheng;Williams, Matthew;Nuss, John M.;Brooks, Eric;Foster, Paul;Goon, Leanne;Heald, Nathan;Holst, Charles;Jaeger, Christopher;Lam, Scott;Lougheed, Julie;Nguyen, Lam;Plonowski, Arthur;Song, Joanne;Stout, Thomas;Wu, Xiang;Yakes, Michael F.;Yu, Peiwen;Zhang, Wentao;Lamb, Peter;Raeber, Olivia [Journal of Medicinal Chemistry,2012,vol. 55,# 11,p. 5467 - 5482] Location in patent:experimental part