9H-Purine, 9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-2,6-dichloro- synthesis

1synthesis methods

Product Name:9H-Purine, 9-(3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-2,6-dichloro-
CAS Number:103884-99-7
Molecular formula:C19H15Cl2FN4O5
Molecular Weight:469.25

Yield:-

Steps:

Multi-step reaction with 2 steps
1: HBr / CH₂Cl₂ / 24 h / 5 °C
2: 4A molecular sieves / 1,2-dichloro-ethane / 16 h / Heating

References:

Montgomery;Shortnacy;Carson;Secrist III [Journal of Medicinal Chemistry,1986,vol. 29,# 11,p. 2389 - 2392]

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